Synthesis of alkyl alkynyl ketones by Pd/light-induced three-component coupling reactions of iodoalkanes, CO, and 1-alkynes
A Fusano, T Fukuyama, S Nishitani, T Inouye…
Index: Organic Letters, , vol. 12, # 10 p. 2410 - 2413
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Citation Number: 69
Abstract
... Volume: Page: Digital Object Identifier (DOI). ... Organic Letters. ... from 200 ml. liquid NH3 and 5.1 g. Na as above) poured into IV with cooling, stirred 1 hr., 24 g. BzH added dropwise, let stand 12 hrs., the NaNH2 decompd. with 75 g. NH4Cl, water added, extd. ...
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