A New Method for the Preparation of 1, 5-Diynes. Synthesis of (4 E, 6 Z, 10 Z)-4, 6, 10-Hexadecatrien-1-ol, the Pheromone Component of the Cocoa Pod Borer Moth …
AR Pereira, JA Cabezas
Index: Journal of Organic Chemistry, , vol. 70, # 7 p. 2594 - 2597
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Citation Number: 24
Abstract
... The Journal of Organic ... with NaOH (3 M, 2 mL) and H 2 O 2 (30%, 2 mL), stirred for 15 min, and extracted with ether (3 × 25 mL), and the organic extracts were ... MHz) δ 0.04 (s, 6H), 0.89 (s, 9H), 1.61 (tt, 2H, J = 7.2, 6.0 Hz), 2.11 (tdd, 2H, J = 7.2, 7.2, 1.2 Hz), 3.61 (t, 2H, J = 6.0 Hz ...
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