Wacker-type oxidation of internal alkenes using Pd (Quinox) and TBHP

RJ DeLuca, JL Edwards, LD Steffens…

Index: Journal of Organic Chemistry, , vol. 78, # 4 p. 1682 - 1686

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Citation Number: 21

Abstract

... The Journal of Organic ... The combined organic layers were then washed with brine (30 mL), dried over Na 2 SO 4 , decanted, and concentrated in vacuo. ... 3H), 1.18–1.37 (m, 10H), 1.99 (q, J = 7.2 Hz 2H), 4.23 (d, J = 6.0 Hz, 2H), 5.50 (dt, J = 15.5, 6.6 Hz, 1H), 5.74 (dt, J = 15.5, 7.1 ...

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