Tetrahedron

Preparation of α-aminophosphines on solid support: model studies and parallel synthesis

BBN Ben-Aroya, M Portnoy

Index: Tetrahedron, , vol. 58, # 25 p. 5147 - 5158

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Citation Number: 16

Abstract

... Tetrahedron. Volume 58, Issue 25, 17 June 2002, Pages 5147–5158. ... X=Cl: (i)t-Boc-Ala-OH, Cs 2 CO 3 , KI (cat.), DMF, 80°C, 24 h; (ii) TFA–CHCl 3 (1:1 vol); (iii) DIPEA, THF; X=Br: (iv) Fmoc-Ala-OH, DIPEA, CsI, DMF, rt, 18 h; (v) 20% piperidine in DMF; (vi) PhCHO, TMOF/DCM ...

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