Organic letters

A new one-pot, four-component synthesis of 1, 2-amino alcohols: TiCl3/t-BuOOH-mediated radical hydroxymethylation of imines

A Clerici, A Ghilardi, N Pastori, C Punta, O Porta

Index: Organic Letters, , vol. 10, # 21 p. 5063 - 5066

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Citation Number: 31

Abstract

... Volume: Page: ... Organic Letters. ... 8 mmol of a 15% aqueous acidic solution) over 30 min at room temperature to a solution containing 1a−d (2 mmol), 2 (7.5 mmol), and TBHP (5 mmol) in 10 mL of methanol under N 2 atmosphere until a pale blue color was barely ...

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