Journal of the American Chemical Society

The synthesis of some isomeric dimethyl-hydroxymethylpyridines. 3, 4-Didesoxypyridoxin

RP Mariella, JL Leech

Index: Mariella; Leech Journal of the American Chemical Society, 1949 , vol. 71, p. 331

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Citation Number: 14

Abstract

Summary The preparation of 2, 2, 5, 5-tetramethyl-3, 6-diketopiperazine (IV) from a- aminoisobutyric acid is described. This diketopiperazine has been converted to 2, 2, 5, 5- tetramethylpiperazine (I) and 2, 2, 5, 5-tetramethyl-3-ketopiperazine (V) by catalytic hydrogenation over copper-chromium oxide as well as by reduction with sodium in butanol.

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