X-ray crystal structure of tribenzylaluminum· diethyl etherate

AFMM Rahman, KF Siddiqui, JP Oliver

Index: Rahman, A. F. M. Maqsudur; Siddiqui, Kaniz F.; Oliver, John P. Journal of Organometallic Chemistry, 1987 , vol. 319, p. 161 - 166

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Citation Number: 17

Abstract

Abstract The crystal structure of tribenzylaluminum· diethyl etherate has been determined by single crystal X-ray diffraction techniques. It crystallizes in the monoclinic system, space group P2 1, with unit cell dimensions of a 8.106 (1), b 15.098 (2), c 10.037 (1) Å, β 111.02 (1), V 1146.6 (3) Å 3, and Z= 2. The final full matrix least-squares refinement on 1139 data gave RF 3.8 and R wF 5.2%. The compound is similar to other organoaluminum adducts ...