Synthetic Communications

Organic Preparations with Molar Amounts of Volatile Malodorous Thiols

D Müller, K Adelsberger, P Imming

Index: Mueller, Diana; Adelsberger, Klaus; Imming, Peter Synthetic Communications, 2013 , vol. 43, # 10 p. 1447 - 1454

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Citation Number: 2

Abstract

Thiols are indispensable for the preparation of many organic sulfur compounds. Their strong smell and use for gas leakage perception render it almost impossible to work with them without arousing public attention. Molar amounts of the very odoriferous thiol 2-methyl-2-propanethiol (t-butylthiol) are needed, for example, for the large-scale synthesis of two useful synthetic building blocks, 1,2,4,5-tetrakis(t-butylthio)benzene and tetramethylbenzo-2,2,6,6-[1,2-d;4,5-d']bis[ ...