Synthesis and Structure of Gold and Platinum Menthyl Complexes

AA Zuzek, SC Reynolds, DS Glueck, JA Golen…

Index: Braddock, D. Christopher; Pouwer, Rebecca H.; Burton, Jonathan W.; Broadwith, Phillip Journal of Organic Chemistry, 2009 , vol. 74, # 16 p. 6042 - 6049

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Abstract

... Quantity minimized: R w (F 2 ) = ∑[w(F o 2 − F c 2 ) 2 ]/∑[(wF o 2 ) 2 ] 1/2 ; R = ∑Δ/∑(F o ), Δ = ∣(F o − F c )∣, w = 1/[σ 2 (F o 2 ) + (aP) 2 + bP], P = [2F c 2 + Max ... The most distinctive feature was the 13 C{ 1 H} NMR signal of the Pt-CH(menthyl) group (δ 43.3 (d, J = 98, C ...

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