Disproportionation of monolithium acetylide into dilithium carbide and acetylene is a reversible reaction in tetrahydrofuran at 0 C

J Mortier, M Vaultier, F Carreaux…

Index: Journal of Organic Chemistry, , vol. 63, # 10 p. 3515 - 3516

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Citation Number: 24

Abstract

... The Chemistry of the Carbon-Carbon Triple Bond; Wiley: New York, 1978 ... The combined organic layer is dried (MgSO4), filtrated, and concentrated in vacuo to give a yellow oil which is purified by Kugelrohr distillation to obtain 1.19 g (90%) of the alcohol as a pale oil ... 3516 J. Org ...

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