Facile Solid??Phase Synthesis of Cycloalkylphosphonates and 1??Cycloalkenylphosphonates Using Polymer??Supported Phenylsulfonylmethylphosphonates

…, SR Sheng, W Zhou, QY Wang, XL Zhang…

Index: Liu, Xiao-Ling; Sheng, Shou-Ri; Zhou, Wei; Wang, Qin-Ying; Zhang, Xiao-Lan; Gong, Bin Synthetic Communications, 2007 , vol. 37, # 1 p. 119 - 127

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Citation Number: 13

Abstract

View all references we herein report the extension of this sulfone??based chemistry to a convenient, traceless, solid??phase synthesis of cycloalkylphosphonates and 1??cycloalkenylphosphonates using polystyrene??supported phenylsulfonylmethylphosphonate. The procedure for the synthesis of target compounds from polystyrene/1% divinylbenzene sodium phenylsulfinate (1) include (a) sulfinate S??alkylation, (b) the sulfonyl anion bis??alkylations with dihaloalkanes, and (c) ...

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