1-Azetine: thermal ring opening to 2-azabutadiene

JC Guillemin, JM Denis…

Index: Guellemin,J.C.; Denis,J.M.; Lablache,A. Journal of the American Chemical Society, 1981 , vol. 103, p. 468

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Citation Number: 32

Abstract

(4) tert-Butyl alcohol formed in the reaction was efficiently eliminated by a dry-ice trap fitted on to the vacuum line after the elimination apparatus.(5) Several grams could be obtained with the same solid base if the addition of chloro amine 1 was regular and slow (1 g/h).(6)'H NMR (CDCIJ 6 4.2 (m, 1 H), 3.6 (m, 2 H), 2.6 (m, 2 H); IR (CD2C12) PN-" 3680, 3595, uGN 2208 cd. Due to the instability of this moduct. combustion analvsis could not be carried out ...

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