The Journal of Organic Chemistry

Reactions of trihalomethylcarbinols with aqueous potassium hydroxide

W Reeve, R Tsuk

Index: Reeve, Wilkins; Tsuk, Ruth Journal of Organic Chemistry, 1980 , vol. 45, # 25 p. 5214 - 5215

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Citation Number: 6

Abstract

Analysis of a-Halophenylacetic Acids? Total halogen was first determined by hydrolyzing 100 mg of the halo acid with 25 mL of 0.5 N sodium hydroxide solution on a stream bath for 30 min. The cold solution was acidified with dilute nitric acid and titrated with 0.02 N silver nitrate with two drops of saturated potassium chromate solution as indicator. Bromine was determined by hydrolyzing a 50-mg sample as above, neutralizing with dilute hydrochloric ...

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