Synthesis and structure of bis [1-(1-adamantyl)-4, 4, 4-trifluorobutane-2, 4-dionato] copper

VK Khamylov, TS Pochekutova, BI Petrov…

Index: Khamylov; Pochekutova; Petrov; Sizov; Fukin; Kurskii; Arapova Russian Journal of General Chemistry, 2009 , vol. 79, # 1 p. 31 - 36

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Abstract

Abstract Previously unknown 1-(1-adamantyl)-4, 4, 4-trifluorobutane-2, 4-dione and its copper complex, bis [1-(1-adamantyl)-4, 4, 4-trifluorobutane-2, 4-dionato] copper, were synthesized. The 1 H NMR, IR, and ESR spectra and X-ray diffraction patterns of the synthesized compounds were obtained. Volatilily and thermal stability of the copper complex were studied by thermogravimetric analysis and differential scanning calorimetry.

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