Synthesis and reactions of perylenecarboxylic acid derivatives. VIII. Synthesis of N-alkyl-3, 4: 9, 10-perylenetetracarboxylic monoanhydride monoimide.

Y Nagao, T Misono

Index: Nagao, Yukinori; Misono, Takahisa Bulletin of the Chemical Society of Japan, 1981 , vol. 54, # 4 p. 1191 - 1194

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Citation Number: 39

Abstract

The condensations of 3, 4: 9, 10-perylenetetracarboxylic dianhydride with alkylamines (isobutyl-, pentyl-, hexyl-, and octylamines) were spectroscopically determined. Under all of the reaction conditions employed, N-alkyl-3, 4: 9, 10-perylenetetracarboxylic monoanhydride monoimide (2a–d)(alkyl= a; isobutyl, b; pentyl, c; hexyl, d; octyl) were obtained. As the reaction proceeded, the yield of 2a–d increased at an initial stage but ...