Journal of the American Chemical Society

Aromatic-Aliphatic Nitro Compounds. II. The Condensation of Nitrophenylnitromethanes with Formaldehyde1

LF Fieser, M Gates

Index: Fieser; Gates Journal of the American Chemical Society, 1946 , vol. 68, p. 2249,2250

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Citation Number: 11

Abstract

Summary X convenient procedure for the preparation of the 2-nitro derivative of a-phenyl-P- nitroethyl nitrate has been found in the condensation of o-nitrobenzaldehyde with nitromethane in the presence of triethylamine, and nitration of the total reaction mixture. The 2, 4-dinitro derivative has been prepared by a similar process. The nitrate esters probably are too labile to merit consideration as explosives.

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