A novel spin-labeled amino acid derivative for use in peptide synthesis:(9-fluorenylmethyloxycarbonyl)-2, 2, 6, 6-tetramethylpiperidine-N-oxyl-4-amino-4-carboxylic …

R Marchetto, S Schreier, CR Nakaie

Index: Marchetto, Reinaldo; Schreier, Shirley; Nakaie, Clovis R. Journal of the American Chemical Society, 1993 , vol. 115, # 23 p. 11042 - 11043

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Citation Number: 143

Abstract

Essentially all previous reports on use of the electron spin resonance (ESR) method1 for the study of proteins and peptides involved coupling of the spin label either to amino acid side chains or to the N-or C-terminal residues. 2 When solid-phase peptide synthesis3 was employed, coupling of spin-labeled amino acids was done exclusively at the amino terminal position. M The synthesis of peptides containing spin labels in residues at internal ...

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