Convenient synthesis of silylketenes from 1-tert-butoxy-2-silylethynes

E Valenti, MA Pericas, F Serratosa

Index: Journal of Organic Chemistry, , vol. 55, # 1 p. 395 - 397

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Citation Number: 34

Abstract

... The combined organic extract was dried over MgSO, and con- centrated in vacuo, and the product was purified by preparative TLC on silica gel. ... (1) For a review on organometallic derivatives of ketenes, see: Moreau, J.-L. In The Chemistry of Ketenes, Allenes ... Page 2. 396 J. Org. ...