The Journal of Organic Chemistry

Lead tetraacetate. VI. Stereochemical studies on the formation of bicyclic ethers from alicyclic primary alcohols

S Moon, BH Waxman

Index: Moon,S.; Waxman,B.H. Journal of Organic Chemistry, 1969 , vol. 34, # 2 p. 288 - 292

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Citation Number: 11

Abstract

Results The alcohols were treated with lead tetraacetate from a 1: 1 to a 1: 2 (R0H: LTA) molar ratio in refluxing benzene from 11 hr to 2 days. The composition of the products was determined by gas chromatography and products were identified by comparison of their ir and nmr spectra and retention times on a gas chromatograph with those of authentic samples. The results are summarized in Scheme I.(1)(a) Part V: S. Moon and PR Clifford, J ...

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