Journal of the American Chemical Society

New preparation for chromyl fluoride and chromyl chloride

GD Flesch, HJ Svec

Index: Flesch, G. D.; Svec, H. J. Journal of the American Chemical Society, 1958 , vol. 80, p. 3189 - 3191

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Citation Number: 18

Abstract

When the chloride preparation was to be used immediately, a modified apparatus was used. The three-piece metal unit was replaced by a corresponding one-piece unit of glass attached to a valve with a glass-to-metal seal. CrOpFt.-Technical trade CrOa was vacuum dried overnight at llOo, then placed in a dry-box where all the handling of the reactants took place. Equal amounts of CrOa and CoFs were finely ground and intimately mixed. The ...