Molecular Architecture. 2.1 Synthesis and Metal Complexation of Heptacyclic Terpyridyl Molecular Clefts
…, A Firestone, ADI Kwok, J Liu, R Ludwig…
Index: Bell, Thomas W.; Cragg, Peter J.; Firestone, Albert; Kwok, Albert D.-I.; Liu, Jia; Ludwig, Richard; Sodoma, Andrej Journal of Organic Chemistry, 1998 , vol. 63, # 7 p. 2232 - 2243
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Citation Number: 18
Abstract
Methods are described for the synthesis of a series of functionalized derivatives of 9-butyl-1, 2, 3, 4, 5, 6, 7, 8-octahydroacridine (9), a building block for several types of highly preorganized host compounds. A key intermediate is 5-benzylidene-9-butyl-2, 3, 5, 6, 7, 8- hexahydroacridin-4 (1 H)-one (23), which can also be used in the syntheses of torands and hydrogen-bonding hexagonal lattice receptors. A tridentate cleft (20), consisting of 2, 2'; 6', ...
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