Perfluoroalkyl isocyanates: general synthesis by the pyrolysis of disilyl esters of hydroxamic acids
WJ Middleton
Index: Middleton, William J. Journal of Organic Chemistry, 1984 , vol. 49, # 23 p. 4541 - 4543
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Citation Number: 12
Abstract
Table I. Yields and Physical Data for Compounds 1-14 product” method yield,* % [a]*Oe~, deg mp, “C R t 'H NMR' 13C NMRf ... 2 3 4 5 6 7 8 9 10 11' 12 13 14' ... A A B B B B B B C C C C ... 558 68, 17” 80, 16” 33 38 22 26 19 16 82 81 60 79 ... 75.0-78.0 92.5-93.5 9 2.5-94.0 oil oil
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