Thermotropic ruthenium (II)-containing metallomesogens based on substituted 1, 10-phenanthroline ligands

…, J Ramaekers, K Driesen, P Nockemann…

Index: Holbrey, John D.; Tiddy, Gordon J. T.; Bruce, Duncan W. Journal of the Chemical Society, Dalton Transactions: Inorganic Chemistry (1972-1999), 1995 , # 11 p. 1769 - 1774

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Citation Number: 28

Abstract

... Select a Journal or Book ... The crude product was purified on a silica column with CHCl 3 /hexane/MeOH (50:50:10) as the eluent ... Since the compound holds solvents firmly, it was dried in a vacuum oven at 50 °C. Yield: 30% (0.50 g). δ H (400 MHz, THF-d 8 ): 0.87 (t, 6H, CH 3 ...