Synthesis and Solid-State Characterization of Self-Assembled Macrocyclic Molecular Rotors of Bis (dithiocarbamate) Ligands with Diorganotin (IV)
A Torres-Huerta, B Rodríguez-Molina, H Höpfl…
Index: Torres-Huerta, Aaron; Rodriguez-Molina, Braulio; Hoepfl, Herbert; Garcia-Garibay, Miguel A. Organometallics, 2014 , vol. 33, # 1 p. 354 - 362
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Citation Number: 11
Abstract
Two bis (dithiocarbamate)(bdtc) metallamacrocyclic compounds, 1 and 2, and the deuterated analogues 1-d 8 and 1-d 20 were readily prepared through self-assembly processes involving the corresponding secondary bis (diamines), with two equivalents each of CS2 and dimethyltin (IV) dichloride. Solid-state characterization using FTIR, PXRD, and TGA indicated that the solid phases of both macrocycles were amorphous solids. For ...
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