Asian Journal of Chemistry

Synthesis of Some Cyclophosphorodiamidates Derivatives of Bis (2-chloroethyl) amine

M Jalalifar, S Khalikov, A Javidan

Index: Jalalifar, Mahdi; Khalikov, Shirinbek; Javidan, Abdollah Asian Journal of Chemistry, 2013 , vol. 25, # 11 p. 5985 - 5988

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Abstract

Abstract Phenyl phosphorodichloridate (1) is readily prepared by reaction of phenol with phosphoryl chloride at low temperature. The crude product is white in colour is subjected to vacuum distillation. However, this reagent reacts only poorly with bis (2-chloroethyl) amine hydrochloride at ambient temperature; thus, an alternative route was sought to aniline and to give 2 and 3, respectively compounds. Compound (3) reacted with aniline and ...

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