Synthesis and structures of gold perfluorophthalimido complexes
…, SJ Lancaster, S Bew, DL Hughes, M Bochmann
Index: Savjani, Nicky; Lancaster, Simon J.; Bew, Sean; Hughes, David L.; Bochmann, Manfred Dalton Transactions, 2011 , vol. 40, # 5 p. 1079 - 1090
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Citation Number: 10
Abstract
Compounds of the new tetrafluorophthalimido anion,[C6F4 (CO) 2N]−, are readily accessible by treatment of tetrafluorophthalimide with either LiNPri2 or mixtures of NEt3 and Me3ECl (E= Si or Sn), to give C6F4 (CO) 2N-X (X= Li 3, SiMe34, and SnMe35). The reaction of the trimethylsilyl derivative 4 with AgF leads cleanly to the ion pair complex [Ag (NCMe) 2][Ag (N (CO) 2C6F4) 2](6· 2MeCN), which contains a linear [Ag {N (CO) 2C6F4} 2]− anion ...
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