Practical Sulfonylation of Amines with 4??Hydroxybenzenesulfonyl Chloride: In Situ Silylation–Desilylation

JI Levin, MT Du, K Park

Index: Levin, Jeremy I.; Du, Mila T.; Park, Kaapjoo Synthetic Communications, 2004 , vol. 34, # 15 p. 2773 - 2781

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Citation Number: 5

Abstract

A one??pot procedure for the efficient sulfonylation of amines with 4??hydroxybenzenesulfonyl chloride involving in situ protection and deprotection of the phenol with N,O??bis(trimethylsilyl) acetamide (BTSA) is presented. ... A one??pot procedure for the efficient sulfonylation of amines with 4??hydroxybenzenesulfonyl chloride involving in situ protection and deprotection of the phenol with N,O??bis(trimethylsilyl)acetamide (BTSA) is presented. ... View all references we ...