The Journal of Organic Chemistry

Oxidation of 2-methyl-4, 5, 6, 7-tetrahydrobenzofuran with m-chloroperbenzoic acid

SB Gingerich, PW Jennings

Index: Gingerich, Samuel B.; Jennings, Paul W. Journal of Organic Chemistry, 1983 , vol. 48, # 15 p. 2606 - 2608

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Citation Number: 15

Abstract

Results and Discussion Synthesis and Reaction of Compound 1. Compound 1 was readily synthesized in five steps (48% yield) by using standard reactions that were slightly modified as noted in the Experimental Section. It reacted more vigorously than the 3-methyl analogue at 0" C to form products 2-4 as is shown in eq 1. A higher yield of 2 (70%) was obtained

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