Hydroxylamine Chemistry. V. Aralkoxyguanidines1

DG Martin, EL Schumann, W Veldkamp…

Index: Martin,D.G. et al. Journal of Medicinal Chemistry, 1965 , vol. 8, p. 456 - 459

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Citation Number: 10

Abstract

July 1965 HYDROXYLAMINE CHEMISTRY. V 459 at room temperature. Solid was removed by filtration and washed with CH2Clz. The filtrate was evaporated to dryness under reduced pressure and the residue was extracted with ether. The ethereal extracts were acidified with HCl in isopropyl alcohol affording 38.2 g. of crude aralkoxyamine hydrochloride, mp 199- 201'dec. Recrystallization (methanol-ethyl acetate) afforded 27.2 g. of analytically pure ...