Some Diethylisopropoxyhalogenosilanes and their Hydrolysis Products1

PA McCusker, CE Greene

Index: McCusker; Greene Journal of the American Chemical Society, 1948 , vol. 70, p. 2808

Full Text: HTML

Citation Number: 4

Abstract

Aug., 1948 DIETHYLISOPROPOXYHALOGENOSILANES AND HYDROLYSIS PRODUCTS 2807 ... (1 : 1) were placed in a one-liter flask. To this was added with rapid stimng, 320 g. (2 moles) of 1-(n-butoxy)ethyl acetate over a period of fifty-five minutes. The tempera- ture was maintained at 10-20' by means of an ice- bath. Stirring was continued for thirty minutes, the re- action mixture poured into a suspension of 106 g. (1.0 mole) of sodium carbonate in 150 ml. of water, the ...