Australian Journal of Chemistry

Some unsymmetrically substituted thiourea derivatives

GW Evans, B Milligan

Index: Evans,G.W.; Milligan,B. Australian Journal of Chemistry, 1967 , vol. 20, p. 185 - 188

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Citation Number: 2

Abstract

N-Acetylbenzylamine was converted into w-acetamidotoluene-p-sulphonyl chloride by reaction with chlorosulphonic acid, using the method described by Smiles and Stewart6 for p- acetamidobenzenesulphonyl chloride. The acid chloride was hydrolysed by heating with water on a steam-bath for 1 hr, and the solution was then neutralized with sodium hydroxide and evaporated to dryness. Crystallization of the residue from aqueous ethanol gave ...

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