The Journal of organic chemistry

Palladium-Catalyzed Heck-type Domino Cyclization and Carboxylation to Synthesize Carboxylic Acids by Utilizing Chloroform as the Carbon Monoxide Source

X Liu, B Li, Z Gu

Index: Priebbenow, Daniel L.; Henderson, Luke C.; Pfeffer, Frederick M.; Stewart, Scott G. Journal of Organic Chemistry, 2010 , vol. 75, # 5 p. 1787 - 1790

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Citation Number: 7

Abstract

... for C 11 H 11 N 2 O 3 INa + (M + Na) + 368.9712, found 368.9709. N-(2-Iodo-5-methoxyphenyl)- N-methylmethacrylamide (1g) 1g (10% ethyl acetate/hexanes) (0.80 g, 80%) was prepared following the procedure of 1d in 3.00 mmol scale. Solid: mp 128.9–132.8 °C (PE/EA). ...

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