Star-porphyrazines: synthetic, structural, and spectral investigation of complexes of the polynucleating porphyrazineoctathiolato ligand

…, KA Andersen, OP Anderson, AGM Barrett…

Index: Velazquez, Christopher S.; Fox, Glenn A.; Broderick, William E.; Andersen, Kevin A.; Anderson, Oren P.; Barrett, Anthony G. M.; Huffman, Brian M. Journal of the American Chemical Society, 1992 , vol. 114, # 19 p. 7416 - 7424

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Citation Number: 85

Abstract

Materials and Methods. THF was distilled from sodium benzophenone ketyl. Chloroform (Burdick & Jackson, amylene-stabilized) was free of ethanol. Water was passed through an ion-exchange column and distilled in a glass Corning Mega-Pure system. All other solvents were reagent grade and were used as supplied. Anhydrous ammonia (Matheson) was ultra- high-purity grade. Silica gel used for chromatography