Acrylate as an Efficient Dimethylamine Trap for the Practical Synthesis of 1-tert-Butyl-4-piperidone via Transamination
JS Amato, JYL Chung, RJ Cvetovich…
Index: Tortolani, David R.; Poss, Michael A. Organic Letters, 1999 , vol. 1, # 8 p. 1261 - 1262
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Citation Number: 10
Abstract
... Furthermore, hindered amines tended to produce bis-amine Michael adducts. figure ... Evaporation of the organic extracts afforded essentially pure 1 in 87% assay yield. ... Chim. Acta 1966, 49, 690−695. [CrossRef], [CAS] Synthesis of 4-chloropiperidines. Fankhauser, R.; Grob, CA ...
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