Chinese Chemical Letters

Microwave promoted rapid dehydration of aldoximes to nitriles using melamine-formaldehyde resin supported sulphuric acid in dry media

R Rezaei, M Karami

Index: Rezaei, Ramin; Karami, Marzeih Chinese Chemical Letters, 2011 , vol. 22, # 7 p. 815 - 818

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Citation Number: 12

Abstract

Abstract A simple and convenient procedure for the synthesis of nitriles by dehydration of aldoxime using supported sulphuric acid on melamine-formaldehyde resin (MFR) under solvent-free condition has been developed. A variety of aromatic and aliphatic aldoximes were converted to the corresponding nitriles. The resin was recovered and reused for subsequent reactions.