8-Alkylthio-10-piperazinodibenzo [b, f] thiepins

…, J Metyšová, J Pomykáček, M Protiva

Index: Jilek; Metysova; Pomykacek; Protiva Collection of Czechoslovak Chemical Communications, 1974 , vol. 39, # 11 p. 3338 - 3351

Full Text: HTML

Citation Number: 13

Abstract

3340 Jilek, Metysova, Pomykacek, Protiva: of alcohols XII with thionyl chloride in the presence of pyridine resulted in 2-(4calkylthiophenylthio) benzyl chlorides XIII (method C). Chlorides XIIIb-XIIId were converted in a reaction with sodium cyanide in aqueous ethanol to nitriles XIVb to XIVd (method D); for the conversion of chloride XIIIe to nitrile XIVe sodium cyanide in dimethylformamide was used. Preparation of the dodecylthio derivatives was ...