The Journal of Organic Chemistry

The synthesis and reactions of N, N'-dicarbalkoxy-N, N'-dialkoxyhydrazines and some observations on carbalkoxylium ions

RJ Crawford, R Raap

Index: Crawford,R.J.; Raap,R. Journal of Organic Chemistry, 1963 , vol. 28, p. 2419 - 2424

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Citation Number: 47

Abstract

To this end we carried out the acid-catalyzed decomposition of I in anhydrous diethyl ether and in the presence of hydroxylic solvents. The high boiling material, obtained from the reaction of I and p-toluenesulfonic acid (either the monohydrate or the anhydrous material) in ethereal solution, mas found to be a mixture of ethyl p-toluenesulfonate and another compound which had a nmr spectrum similar to ethyl p-toluenesulfonate but which ...