Preparation of 2, 3-dihydroselenolo [2, 3-b] pyridines and related compounds by free-radical means

T Fenner, JM White, CH Schiesser

Index: Organic and Biomolecular Chemistry, , vol. 4, # 3 p. 466 - 474

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Citation Number: 19

Abstract

... 6b,7 Hydroxyl radicals are extremely reactive and can cause damage to important biomolecules that include ... NaCl (40 mL) and the organic phase dried (MgSO 4 ). Flash chromatography (50% EtOAc ... The combined organics were dried (MgSO 4 ) and concentrated under vacuum ...