Synthesis, composition, and properties of products formed in interaction of ortho-tert-butylphenol with sulfur monochloride
…, NI Komarova, VG Vasil'ev, LM Pokrovskii
Index: Krysin; Egorova; Komarova; Vasil'Ev; Pokrovskii Russian Journal of Applied Chemistry, 2009 , vol. 82, # 11 p. 1965 - 1969
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Abstract
Abstract Interaction of ortho-tert-butylphenol with sulfur monochloride in dimethylformamide leads to an increase in the fraction of phenol di-and polysulfides in the product. Liquid chromato-mass-spectrometry was used to determine the composition of the main groups of compounds contained in the mixture. A number of its components was isolated and produced by counter synthesis.