Serendipitous two-step synthesis of a naphth [3, 2, 1-cd] indole

MJ Kornet, AP Thio, LM Tolbert

Index: Kornet; Milton J.; Thio, Alan P.; Tolbert, Laren M. Journal of Organic Chemistry, 1980 , vol. 45, # 1 p. 30 - 32

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Citation Number: 3

Abstract

Figure 2. Conipound 5 showing proton chemical shifts derived from computer simulation. spectrum. Decoupling experiments and NMR simulation allowed a complete assignment of all chemical shifts and coupling constants, which are listed in Table I. The aromatic region consisted of two independent ABC patterns. Simultaneous simulation of the six-spin system by using the available first-order coupling constants as the initial values gave, after ...