Ozonolysis in Flow Using Capillary Reactors

…, A Ghaini, A Constantinou, A Cantu-Perez…

Index: Roydhouse, M. D.; Motherwell, W. B.; Ghaini, A.; Constantinou, A.; Cantu-Perez, A.; Gavriilidis, A. Organic Process Research and Development, 2011 , vol. 15, # 5 p. 989 - 996

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Citation Number: 17

Abstract

Reactions of n-decene with ozone and subsequent quenching of the formed ozonides were carried out under flow conditions using the standard Vapourtec flow system equipped with a cooled flow cell. The reactions were performed continuously and in the annular flow regime within the circular cross-section channels. Typical flow rates were 0.25–1 mL min–1 for liquid and 25–100 mL min–1 for gas, reactor volumes were 0.07–10 mL formed of 1 mm ...