Insecticidal 1-(alkynylalkyl)-3-cyano-2, 6, 7-trioxabicyclo [2.2. 2] octanes

…, TC Budd, J Sills, JE Casida

Index: Smith, Ian H.; Budd, Timothy C.; Sills, Jill; Casida, John E. Journal of Agricultural and Food Chemistry, 1993 , vol. 41, # 7 p. 1114 - 1117

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Abstract

MATERIALS AND METHODS Spectroscopy. Proton nuclear magnetic resonance (NMR) spectra were recorded at 250 MHz with a Bruker AM-260 spectrometer for samples dissolved in deuteriochloroform. Mass spectra (MS) after chemical ionization (methane at 0.5 Torr) were recorded on a Finnigan 4600 mass spectrometer connected to the output of a gas-phase chromatography column (DB17, 15-m capillary).

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