Bromoalkoxystyrenes1

TL Jacobs, WR Scott Jr

Index: Jacobs; Scott Journal of the American Chemical Society, 1953 , vol. 75, p. 5500,5502

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Citation Number: 6

Abstract

Anal. Calcd. for (GH8O) z: C, 81.79; H, 6.10; mol. wt., 264.3. Found: C, 81.64; H, 5.79; mol. wt.(Rast), 240. Phenylethoxyacetylene.-Using the directions for phenylmethoxyacetylene, 25- to 30-g. samples of bromoethoxystyrenel3 were treated with powdered potassium hydroxide to give 30-35y0 yields of crude material, bp 60-70'(1 mm.). Analysis of this distillate by hydrogenation over Raney nickel and quantitative saponification of the saturated solution ...