Solution??and solid??state structures of N??desmethylnefopam hydrochloride, a metabolite of the analgesic drug
…, J Blumenfeld, D Donnell, N Sugisaka…
Index: Glaser; Geresh; Blumenfeld; Donnell; Sugisaka; Drouin; Michel Journal of Pharmaceutical Sciences, 1993 , vol. 82, # 3 p. 276 - 281
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Citation Number: 9
Abstract
Abstract The solid-state structure of (±)-N-desmethylnefopam hydrochloride (1), a metabolite of the analgesic drug, was determined by single-crystal X-ray diffraction analysis. Compound 1 gave crystalline prisms belonging to the orthorhombic Pcab space group, and at ambient temperature (293 K), a= 9.939 (2), b= 14.479 (1), c= 20.148 (3) A, V= 2899.5 (8) A 3, Z= 8, R (F)= 0.045, and R w (F)= 0.025. The benzoxazocine ring of crystalline 1 is ...
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