Journal of the American Chemical Society

Chlorination of Butyl Trichloroacetates

HM Waddle, H Adkins

Index: Waddle; Adkins Journal of the American Chemical Society, 1939 , vol. 61, p. 3363

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Citation Number: 7

Abstract

CeHs Experimental Reagents.-Anthrone, prepared from anthraquinone,S was reduced to anthracene according to Martin's direc- tions.6 The anthracene crystallized as plates which melted at 216-216.5" (corr.) and which showed a deep purple fluorescence. Commercial dioxane was purified according to the directions of Scatchard and Benedict,' bp 100.5-101 (corr.). Bromine was purified as before.' The purified dioxane did not react with this bromine, even up to ...