The Journal of Organic Chemistry

Convenient synthesis of 3-[1-(phenylthio) alkyl]-and 3-alkyl-substituted 3-sulfolenes

HH Tso, TS Chou, YL Lai

Index: Tso, Hsi-Hwa; Chou, Ta-shue; Lai, Yu-Ling Journal of Organic Chemistry, 1989 ,  vol. 54,  # 17  p. 4138 - 4141

Full Text: HTML

Citation Number: 16

Abstract

34 l-(Phenylthio) alkyl]-3-sulfolenes (5) were conveniently synthesized by a sequence of mesylation, elimination, and Michael addition reactions of 4-hydroxyalkylated 2-sulfolenes (2), which were prepared regioselectively via ultrasound-promoted allylzincation of 4-bromo-