Regioselective synthesis of halohydrin esters from epoxides: reaction with acyl halides and rhodium-catalyzed three-component coupling reaction with alkyl halides …
K Nakano, S Kodama, Y Permana…
Index: Nakano, Koji; Kodama, Shunsuke; Permana, Yessi; Nozaki, Kyoko Chemical Communications, 2009 , # 45 p. 6970 - 6972
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Abstract
Halohydrin esters can be used as building blocks for the synthesis of lipids 1 and biologically active compounds. 2 One of the common synthetic strategies for them is the conversion of 1,2-diols. 3 Another class of powerful synthetic strategies includes using epoxides as a starting material. For example, epoxides can be transformed into halohydrin esters via a two-step procedure in one-pot: (i) the ring-opening by halogen nucleophiles and (ii) the subsequent ...
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