Journal of Pharmaceutical and Biomedical Analysis 1997-02-01

Development and validation of a general non-digestive method for the determination of palladium in bulk pharmaceutical chemicals and their synthetic intermediates by graphite furnace atomic absorption spectroscopy.

T Wang, S Walden, R Egan

Index: J. Pharm. Biomed. Anal. 15(5) , 593-9, (1997)

Full Text: HTML

Abstract

A simple, selective, sensitive, accurate and relatively inexpensive method for the determination of palladium in bulk pharmaceutical chemicals (BPC) and their synthetic intermediates by graphite furnace atomic absorption spectroscopy has been developed and validated. Sample preparation by direct dissolution of sample in 70% nitric acid is simple and effective without adverse effects. The limit of detection and the limit of quantitation of the method were determined to be 0.7 ppm and 2 ppm respectively in BPC.

Related Compounds

  • Dicyclohexylamine
  • Dicyclohexylamine...

Related Articles:

Evaluation of quadrupole-time-of-flight mass spectrometry in comprehensive two-dimensional gas chromatography.

2014-10-03

[J. Chromatogr. A. 1362 , 262-9, (2014)]

Synthesis and application of ionic liquid matrices (ILMs) for effective pathogenic bacteria analysis in matrix assisted laser desorption/ionization (MALDI-MS).

2013-03-12

[Anal. Chim. Acta 767 , 104-11, (2013)]

Retention time prediction of compounds in Grob standard mixture for apolar capillary columns in temperature-programmed gas chromatography.

2009-01-01

[Anal. Bioanal. Chem 393(1) , 327-34, (2009)]

Studies on antifungal properties of phenol complexes with secondary amines. 1. The effect of complex formation of nitro- and chlorophenols with dicyclohexylamine on the antifungal activity in vitro.

1989-07-01

[Mycoses 32(7) , 359-61, (1989)]

Effect of drugs inhibiting spermidine biosynthesis and metabolism on the in vitro development of Plasmodium falciparum.

2001-11-01

[Parasitol. Res. 87(11) , 963-72, (2001)]

More Articles...