Journal of AOAC International 1993-01-01

Gas chromatographic determination of benalaxyl residues in different crops and water.

T Crisippi, G Zini, R Fabbrini

Index: J. AOAC Int. 76(3) , 650-6, (1993)

Full Text: HTML

Abstract

A gas chromatographic method is described that is suitable for the determination of benalaxyl residues ranging from 10 to 0.1 micrograms/kg in several crops, must, wine, and water. The compound is extracted with acetone and purified either by partitioning between water and n-hexane or by passing the extract through an Extrelut column with n-hexane. Further purification is achieved by column chromatography on alumina. The active ingredient is finally determined by gas chromatography with nitrogen-phosphorus detection. Mean recoveries were > or = 95% in the various crops tested and in the 0.01-1.05 mg/kg fortification range. Standard deviations for each crop were < or = 6.5%.

Related Compounds

  • Benalaxyl-M
  • benalaxyl

Related Articles:

High-throughput electrophoretic mobility shift assays for quantitative analysis of molecular binding reactions.

2014-10-21

[Anal. Chem. 86(20) , 10357-64, (2014)]

Formulation approaches to improving the delivery of an antiviral drug with activity against seasonal flu.

2015-03-01

[Pharm. Dev. Technol. 20(2) , 169-75, (2015)]

Purification and characterization of a DNA-binding recombinant PREP1:PBX1 complex.

2015-01-01

[PLoS ONE 10(4) , e0125789, (2015)]

Erythroid induction of K562 cells treated with mithramycin is associated with inhibition of raptor gene transcription and mammalian target of rapamycin complex 1 (mTORC1) functions.

2015-01-01

[Pharmacol. Res. 91 , 57-68, (2015)]

Enhancement of enzymatic colorimetric response by silver island films on high throughput screening microplates.

2014-09-01

[J. Immunol. Methods 411 , 43-9, (2014)]

More Articles...