The Journal of organic chemistry

A convenient and highly chemoselective method for the reductive acetylation of azides

T Rosen, IM Lico, DTW Chu

Index: Rosen, Terry; Lico, Isabella M.; Chu, Daniel T. W. Journal of Organic Chemistry, 1988 , vol. 53, # 7 p. 1580 - 1582

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Citation Number: 186

Abstract

88-90 oil lectivity associated with the preparation of the precursor azides. Thus, the reduction represents a pivotal step in a stereoselective sequence for the preparation of amines. Several methods and reagents are available for this transformation that is often carried out by catalytic hydr~ genation~,~ or by treatment with lithium aluminum h~ dride.~ Other known procedures include H2S/pyridine/H20, 4 transfer hydrogenation: Ph3P, GH,/ ...

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